data_Sb2OsRu
_symmetry_space_group_name_H-M   'P 1'
_cell_length_a   4.71
_cell_length_b   4.71
_cell_length_c   3.19
_cell_angle_alpha   90.0
_cell_angle_beta   90.0
_cell_angle_gamma   95.35
_symmetry_Int_Tables_number   1
_chemical_formula_structural   Sb2OsRu
_chemical_formula_sum   'Sb2 Os1 Ru1'
_cell_volume   70.48
_cell_formula_units_Z   1
loop_
 _symmetry_equiv_pos_site_id
 _symmetry_equiv_pos_as_xyz
  1  'x, y, z'
loop_
 _atom_site_type_symbol
 _atom_site_label
 _atom_site_symmetry_multiplicity
 _atom_site_fract_x
 _atom_site_fract_y
 _atom_site_fract_z
 _atom_site_occupancy
  Sb  Sb2  1  0.59  0.74  0.59  1.0
  Sb  Sb3  1  0.59  0.26  0.59  1.0
  Os  Os0  1  0.17  0.0  0.0  1.0
  Ru  Ru1  1  0.0  0.0  0.0  1.0

data_Sb2OsRu
_symmetry_space_group_name_H-M   P1
_cell_length_a   3.19
_cell_length_b   4.71
_cell_length_c   4.71
_cell_angle_alpha   95.35
_cell_angle_beta   90.0
_cell_angle_gamma   90.0
_symmetry_Int_Tables_number   1
_chemical_formula_structural   Sb2OsRu
_chemical_formula_sum   'Sb2 Os1 Ru1'
_cell_volume   70.48
_cell_formula_units_Z   1
loop_
 _symmetry_equiv_pos_site_id
 _symmetry_equiv_pos_as_xyz
  1  'x, y, z'
loop_
 _atom_site_type_symbol
 _atom_site_label
 _atom_site_symmetry_multiplicity
 _atom_site_fract_x
 _atom_site_fract_y
 _atom_site_fract_z
 _atom_site_occupancy
  Sb  Sb0  1  0.59  0.59  0.26  1.0
  Sb  Sb1  1  0.59  0.59  0.74  1.0
  Ru  Ru2  1  0.0  0.0  0.0  1.0
  Os  Os3  1  0.0  0.17  0.0  1.0

Sb Sb Os Ru
Sb Sb Os Ru 0 2 o + + 0 1 o + o 0 1 o o o 0 3 + + o 0 3 + + + 1 2 o o o 1 2 o o + 1 3 + o + 2 3 o o o 
OsRuSb2 crystallizes in the triclinic P1 space group. Os(1) is bonded in a 1-coordinate geometry to one Ru(1), two equivalent Sb(1), and two equivalent Sb(2) atoms. The Os(1)-Ru(1) bond length is 0.81 Å. There is one shorter (2.72 Å) and one longer (3.05 Å) Os(1)-Sb(1) bond length. There is one shorter (2.55 Å) and one longer (2.90 Å) Os(1)-Sb(2) bond length. Ru(1) is bonded in a 1-coordinate geometry to one Os(1), two equivalent Sb(1), and two equivalent Sb(2) atoms. There is one shorter (2.55 Å) and one longer (2.90 Å) Ru(1)-Sb(1) bond length. There is one shorter (2.72 Å) and one longer (3.05 Å) Ru(1)-Sb(2) bond length. There are two inequivalent Sb sites. In the first Sb site, Sb(1) is bonded in a 8-coordinate geometry to two equivalent Os(1), two equivalent Ru(1), two equivalent Sb(1), and two equivalent Sb(2) atoms. Both Sb(1)-Sb(1) bond lengths are 3.19 Å. There is one shorter (2.28 Å) and one longer (2.43 Å) Sb(1)-Sb(2) bond length. In the second Sb site, Sb(2) is bonded in a 8-coordinate geometry to two equivalent Os(1), two equivalent Ru(1), two equivalent Sb(1), and two equivalent Sb(2) atoms. Both Sb(2)-Sb(2) bond lengths are 3.19 Å.